Mariosimone Zoccali

Mariosimone Zoccali is an assistant professor of analytical chemistry in the Department of Mathematical and Computer Science, Physical Sciences and Earth Sciences at the University of Messina, in Italy since July 2019. His research is focused on the development of multidimensional chromatographic instrumentation and software (GC×GC, LC–GC, LC–GC×GC, SFE–SFC), coupled to state-of-the-art MS for the study of complex matrices constituents and contaminants. Mariosimone has authored or co-authored more than 65 articles and book chapters. He has given award-winning presentations at multiple international meetings. He has been directly involved with the development of award-winning instrumentation. In particular, he assembled a five-dimensional instrument consisting of a liquid chromatography system combined with a comprehensive two-dimensional gas chromatography-triple quadrupole mass spectrometry instrument. Zoccali received recognition for his achievements in 2018 with the “Young Researcher Award”, on behalf of the Interdivisional Separation Science Group (Italian Society of Chemistry), in 2021 he has been nominated “Rising Stars of Separation Science” by the journal “Columns” and won the “Young Researcher Award”, on behalf of the Italian Analytical Chemistry Division of the (Italian Society of Chemistry). In 2022 won the “John B. Phillips Award” conferred during the 19th International GC×GC Symposium. He has pursued and won multiple travel awards to better disseminate his research to the broader scientific community. He is also leader of the working group three of the EuChemS-DAC Sample Preparation Study Group.


1.     Peter Quinto Tranchida, Mariosimone Zoccali, Giorgia Purcaro, Sabrina Moret, Lanfranco Conte, Marco Beccaria, Paola Dugo, Luigi Mondello.

A rapid multidimensional liquid-gas chromatography method for the analysis of mineral oil saturated hydrocarbons in vegetable oils.

J. Chromatogr. A 2011; 1218:7476-80.


2.     Peter Q. Tranchida, Mariosimone Zoccali, Paola Dugo, and Luigi Mondello

Rapid multidimensional liquid-gas chromatography for the analysis of saturated hydrocarbon contamination in foods containing vegetable oil.

LC-GC Europe 2012 25(4):20-25.


3.     Luigi Mondello, Mariosimone Zoccali, Giorgia Purcaro, Flavio Antonio Franchina, Danilo Sciarrone, Sabrina Moret, Lanfranco Conte, Peter Quinto Tranchida.                                                                       

Determination of saturated-hydrocarbon contamination in baby foods by using on-line liquid–gas chromatography and off-line liquid chromatography-comprehensive gas chromatography combined with mass spectrometry.

J. Chromatogr. A 2012 1259:221-226.


4.     Peter Quinto Tranchida, Mariosimone Zoccali, Flavio Antonio Franchina, Paola Dugo, Luigi Mondello.

Measurement of fundamental chromatography parameters in conventional and split-flow comprehensive two-dimensional gas chromatography-mass spectrometry: a focus on the importance of second-dimension injection efficiency.

J. Sep. Sci. 2013 36:212-218.


5.     Giorgia Purcaro, Mariosimone Zoccali, Peter Quinto Tranchida, Laura Barp, Sabrina Moret, Lanfranco Conte, Paola Dugo, Luigi Mondello. 

Comparison of two different multidimensional liquid-gas chromatography interfaces for the determination of mineral oil saturated hydrocarbon in foodstuff.                                                                                                                         

Anal. Bioanal. Chem. 2013; 405:1077-1084.


6.     Peter Quinto Tranchida, Mariosimone Zoccali, Flavio Antonio Franchina, Ivana Bonaccorsi, Paola Dugo, Luigi Mondello. 

Fast gas chromatography combined with a high-speed triple quadrupole mass spectrometer for the analysis of unknown and target citrus essential oil volatiles.

J. Sep. Sci. 2013; 36:511-516. 


7.     Peter Quinto Tranchida, Flavio Antonio Franchina, Mariosimone Zoccali, Sebastiano Pantò, Danilo Sciarrone, Paola Dugo, Luigi Mondello.

Untargeted and targeted comprehensive two-dimensional GC analysis using a novel unified high-speed triple quadrupole mass spectrometer.

J. Chromatogr. A 2013; 1278:153-159. 


8.     Peter Quinto Tranchida, Mariosimone Zoccali, Luisa Schipilliti, Danilo Sciarrone, Paola Dugo, Luigi Mondello.                                                                                                                      

Solid-phase microextraction-fast gas chromatography combined with a high-speed triple quadrupole mass spectrometer for targeted and untargeted food analysis.

J. Sep. Sci. 2013 36:2145-2150. 


9.     Peter Quinto Tranchida, Flavio Antonio Franchina, Mariosimone Zoccali, Ivana Bonaccorsi, Francesco Cacciola, Luigi Mondello.

A direct sensitivity comparison between flow-modulated comprehensive 2- and 1-D GC in untargeted and targeted MS based experiments.

      J. Sep. Sci. 2013 36:2746-2752.


10.  Peter Quinto Tranchida, Mariosimone Zoccali, Ivana Bonaccorsi, Paolo Dugo, Luigi Mondello, Giovanni Dugo.

The Off-Line Combination Of High Performance Liquid Chromatography And

Comprehensive Two-Dimensional Gas Chromatography-Mass Spectrometry: A Powerful Approach For Highly-Detailed Essential Oil Analysis

J. Chromatogr. A 2013 1305:276-284. 


11.  Peter Q. Tranchida, Mariosimone Zoccali, Flavio A. Franchina, Antonella Cotroneo, Paolo Dugo, Luigi Mondello.                                                                                                                                                                

Gas velocity at the point of re-injection: an additional parameter in comprehensive two-dimensional gas chromatography optimization.

J. Chromatogr. A 2013 1314:216-223. 


12.  Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello. 

On-Line Combination of High Performance Liquid Chromatography with Comprehensive Two-         Dimensional Gas Chromatography-Triple Quadrupole Mass Spectrometry: A Proof of Principle Study. 

Anal. Chem. 2015 87:1911-1918. 


13.  Laura Barp, Giorgia Purcaro, Flavio A. Franchina, Mariosimone Zoccali, Danilo Sciarrone, 

Q. Tranchida, Luigi Mondello. 

Determination of phthalate esters in vegetable oils using direct immersion solid-phase microextraction and fast gas chromatography coupled with triple quadrupole mass spectrometry.

Analytica Chimica Acta 2015 887:237-244. 


14.  Mariosimone Zoccali, Ivana L. Bonaccorsi, Peter Q. Tranchida, Paola Dugo, Luigi Mondello, Giacomo Dugo. 

Analysis of the sesquiterpene fraction of citrus essential oils by using the off-line combination 

of high performance liquid chromatography and gas chromatography-based methods: a comparative study. 

Flavour Fragr. J. 2015, 30, 411–422.


15.  Mariosimone Zoccali, Laura Barp, Marco Beccaria, Danilo Sciarrone, Giorgia Purcaro, Luigi Mondello. 

Improvement of mineral oil saturated and aromatic hydrocarbons determination in edible oil by liquid-liquid-gas chromatography with dual detection.

J. Sep. Sci. 2015 39, 623-631.


16.  Mariosimone Zoccali, Peter Q. Tranchida, Ivana L. Bonaccorsi, Paola Dugo, Luigi Mondello, Giovanni Dugo. 

Detailed Profiling of the Volatile Oxygenated Fraction of Mandarin Essential Oils by Using the Off Line Combination of High-Performance Liquid Chromatography and Comprehensive Two-Dimensional Gas Chromatography-Mass Spectrometry.

Food Anal. Method 2017 10, 1106-1116.


17.  Mariosimone Zoccali, Giorgia Purcaro, Schepis Antonino, Peter Quinto Tranchida, Luigi Mondello. 

Miniaturization of the QuEChERS Method in the Fast Gas Chromatography-Tandem Mass Spectrometry Analysis of Pesticide Residues in Vegetables.

Food Anal. Method. 2017 10, 2636-2645.


18.  Mariosimone Zoccali, Kevin A. Schug, Phillip Walsh, Jonathan Smuts, Luigi Mondello. 

Flow-modulated comprehensive two-dimensional gas chromatography combined with a vacuum ultraviolet detector for the analysis of complex mixtures.

J. Chromatogr. A 2017 1497, 135-143.


19.  Daniele Giuffrida, Mariosimone Zoccali, Paola Dugo, Luigi Mondello. 

Apocarotenoids determination in Capsicum chinense Jacq. cv. Habanero, by supercritical fluid chromatography-triple-quadrupole/mass spectrometry.

Food Chem. 2017 231, 316-323.


20.  Mariosimone Zoccali, Daniele Giuffrida, Paola Dugo, Luigi Mondello. 

Direct online extraction and determination by supercritical fluid extraction-chromatography-mass spectrometry of targeted carotenoids from red Habanero peppers (Capsicum chinense Jacq.).

Journal of Separation Science. 2017 40, 3905-3913. 


21.  Danilo Sciarrone, Daniele Giuffrida, Archimede Rotondo, Giuseppe Micalizzi, Mariosimone Zoccali, Sebastiano Pantò, Paola Donato, Rosana Goncalves Rodrigues-das-Dores, Luigi Mondello. 

Quali-quantitative characterization of the volatile constituents in Cordia verbenacea D.C. essential oil exploiting advanced chromatographic approaches and nuclear magnetic resonance analysis. J. Chromatogr. A. 2017; 1524, 246-253.


22.  Mariosimone Zoccali, Simone Cappello, Luigi Mondello. 

Multilevel characterization of marine microbial biodegradation potentiality by means of flow-modulated comprehensive two-dimensional gas chromatography combined with a triple quadrupole mass spectrometer.

J. Chromatogr. A. 2018; 1547, 99-106. 


23.  Daniele Giuffrida, Mariosimone Zoccali, Adriana Arigò, Francesco Cacciola, Coralia Osorio Roa, Paola Dugo, Luigi Mondello. 

Comparison of different analytical techniques for the analysis of carotenoids in tamarillo (Solanum betaceum Cav.).

Arch. Biochem. Biophys. 2018; 646, 161-167.


24.  Marina Russo, Paola Dugo, Chiara Fanali, Laura Dugo, Mariosimone Zoccali, Luigi Mondello, Laura De Gara. 

Use of an Online Extraction Technique Coupled to Liquid Chromatography for Determination of Caffeine, Tea, Cocoa.

Food Anal. Method. 2018; 11, 2637-2644.


25.  Mariosimone Zoccali, Adriana Arigò, Marina Russo, Fabio Salafia, Paola Dugo, Luigi Mondello.

Characterization of Limonoids in Citrus Essential Oils by Means of Supercritical Fluid Chromatography Tandem Mass Spectrometry.

Food Anal. Method. 2018; 11, 3257-3266.


26.  Danilo Sciarrone, Antonino Schepis, Mariosimone Zoccali, Paola Donato, Federico Vita, Donato Creti, Amedeo Alpi, Luigi Mondello.

Multidimensional Gas Chromatography Coupled to Combustion-Isotope Ratio Mass Spectrometry/Quadrupole MS with a Low-Bleed Ionic Liquid Secondary Column for the Authentication of Truffles and Products Containing Truffle.

Anal. Chem. 2018 90, 6610-6617.


27.  Mariosimone Zoccali, Daniele Giuffrida, Fabio Salafia, Salvatore Vincenzo Giofrè, Luigi Mondello.

Carotenoids and apocarotenoids determination in intact human blood samples by online supercritical fluid extraction-supercritical fluid chromatography-tandem mass spectrometry.

Anal. Chim. ACTA 2018; 1032, 40-47.


28.  Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello.

On-line liquid chromatography-comprehensive two dimensional gas chromatography with dual detection for the analysis of mineral oil and synthetic hydrocarbons in cosmetic lip care products.

Anal. Chim. ACTA 2019; 1048, 221-226.


29.  Mariosimone Zoccali, Barbara Giocastro, Peter Q. Tranchida, Luigi Mondello.

Use of a recently developed thermal modulator within the context of comprehensive two-dimensional gas chromatography combined with time-of-flight mass spectrometry: Gas flow optimization aspects.

J. Sep. Sci. February 2019: 42, 637-778


30.   Peter Q. Tranchida, Ivan Aloisi, Barbara Giocastro, Mariosimone Zoccali, Luigi Mondello.

Comprehensive two-dimensional gas chromatography-mass spectrometry using milder electron ionization conditions: A preliminary evaluation.

J. Chromatogr. A 2019: 1589, 134-140.


31.   Arena Katia, Cacciola Francesco, Mangraviti Domenica, Mariosimone Zoccali, Rigano Francesca,  

 Marino Nino, Dugo Paola, Luigi Mondello.

Determination of the polyphenolic fraction of Pistacia vera L. kernel extracts by comprehensive two-dimensional liquid chromatography coupled to mass spectrometry detection.

Anal. Bioanal. Chem. 2019: 411, 4819-4829. 


32.  Mariosimone Zoccali, Paola Donato, Luigi Mondello.

Recent advances in the coupling of carbon dioxide-based extraction and separation techniques.

TRAC-Trend. Anal. Chem. 2019: 116, 158-165.


33.  Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello.

Fast Gas Chromatography-Mass Spectrometry: A Review Of The Last Decade.

TRAC-Trend. Anal. Chem. 2019: 118: 444-452.


34.  Mariosimone Zoccali, Daniele Giuffrida, Fabio Salafia, Carmen Socaciu, Kari Skjånes, Paola Dugo, Luigi Mondello.

First Apocarotenoids Profiling of Four Microalgae Strains.

Antioxidants 2019: 8(7), 209, 1-10.


35.  Mariosimone Zoccali, Barbara Giocastro, Ivana L. Bonaccorsi, Alessandra Trozzi, Peter Q. Tranchida, Luigi Mondello.

In-Depth Qualitative Analysis of Lime Essential Oils Using the Off-Line Combination of Normal Phase High Performance Liquid Chromatography and Comprehensive Two-Dimensional Gas Chromatography-Quadrupole Mass Spectrometry.

Foods 2019: 8(11), 580, 1-10.


36.  Daniella C. Murador, Fabio Salafia, Mariosimone Zoccali, Paula L. G. Martins, Antônio G. Ferreira, Paola Dugo, Luigi Mondello, Veridiana V. de Rosso, Daniele Giuffrida.

Green Extraction Approaches for Carotenoids and Esters: Characterization of Native Composition from Orange Peel.

Antioxidants 2019: 8, 613, 1-18.


37.  Mariosimone Zoccali, Daniele Giuffrida, Roberta Granese, Fabio Salafia, Paola Dugo, Luigi Mondello.

Determination of free apocarotenoids and apocarotenoid esters in human colostrum.

Anal. Bioanal. Chem 2020: 412:1335–1342.


38.  Ivan Aloisi, Tiago Schena, Barbara Giocastro, Mariosimone Zoccali, Peter Q. Tranchida, Elina Bastos Caramão, Luigi Mondello.

Towards the determination of an equivalent standard column set between cryogenic and flow-modulated comprehensive two-dimensional gas chromatography.

Anal. Chim. ACTA 2020: 1105, 231-236.


39.  Federico Vita, Beatrice Giuntoli, Edoardo Bertolini, Cosimo Taiti, Elettra Marone, Chiara D’Ambrosio, Emanuela Trovato, Danilo Sciarrone, Mariosimone Zoccali, Raffaella Balestrini, Andrea Scaloni, Luigi Mondello, Stefano Mancuso, Massimo Alessio, Amedeo Alpi.

Tuberomics: A molecular profiling for the adaption of edible fungi (Tuber magnatum Pico) to different natural environments.

BMC Genomics 2020:21, 1-25.


40.  Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello.

A lab-developed interface for liquid-gas chromatography coupling based on the use of a modified programmed-temperature-vaporizing injector.

Journal of Chromatography A 2020:1622, 1-6.   


41.  Ivan Aloisi, Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello.

Analysis of Organic Sulphur Compounds in Coal Tar by Using Comprehensive Two-Dimensional Gas Chromatography-High Resolution Time-of-Flight Mass Spectrometry.

Separations 2020:7, 26, 1-9.


42.  Ivan Aloisi, Mariosimone Zoccali, Paola Dugo, Peter Q. Tranchida, Luigi Mondello.

Fingerprinting of the unsaponifiable fraction of vegetable oils by using cryogenically-modulated comprehensive two-dimensional gas chromatography-high resolution time-of-flight mass spectrometry.

Food Anal. Method. 2020:13, 1523-1529.


43.  Mariosimone Zoccali, Daniele Giuffrida, Fabio Salafia, Francesca Rigano, Paola Dugo, Monica Casale, Luigi Mondello.

Apocarotenoids profiling in different Capsicum species.

Food Chemistry. 2021:334, 127595.


44.  Barbara Giocastro, Ivan Aloisi, Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello.

Cryogenic- and Flow-Modulation Comprehensive Two-Dimensional Gas Chromatography–

Mass Spectrometry: Obtaining Similar Chromatographic Performances.

LC-GC North America. 2020:38, 548-558.


45.  Daniele Giuffrida, Mariosimone Zoccali, Luigi Mondello.

Recent developments in the carotenoid and carotenoid derivatives chromatography-mass spectrometry analysis in food matrices.

TRAC-Trend. Anal. Chem. 2020:132, 1160474.


46.  Benedikt A. Weggler, Lena M. Dubois, Nadine Gawlitta, Thomas Gröger, John Moncur, Luigi Mondello, Steven Reichenbach, Peter Tranchida, Zhijun Zhao, Ralf Zimmermann, Mariosimone Zoccali, Jean-François Focant.

A unique data analysis framework and open source benchmark data set for the analysis of comprehensive two-dimensional gas chromatography software.

J. Chromatogr. A 2021:1635, 461721.


47.  Barbara Giocastro, Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello.

Evaluation of different internal diameter coated modulation columns within the context of solid-state modulation.

J. Sep. Sci. 44 (2021) 1923–1930.


48.  Giuseppe Micalizzi, Filippo Alibrando, Federica Vento, Emanuela Trovato, Mariosimone Zoccali, Paolo Guarnaccia, Paola Dugo, Luigi Mondello.

Development of a Novel Microwave Distillation Technique for the Isolation of Cannabis sativa L. Essential Oil and Gas Chromatography Analyses for the Comprehensive Characterization of Terpenes and Terpenoids, Including Their Enantio-Distribution.

Molecules 2021:26, 1588.


49.  Ivan Aloisi, Barbara Giocastro, Antonio Ferracane, Tania M.G. Salerno, Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello.  

Preliminary observations on the use of a novel low duty cycle flow modulator for comprehensive two-dimensional gas chromatography.

J. Chromatogr. A, 1643, 462076 (2021). 


50.  Antonio Ferracane, Mariosimone Zoccali, Tania Maria Grazia Salerno, Peter Q. Tranchida, Luigi Mondello

Determination of multi-pesticide residues in vegetable products using a “reduced-scale” Quechers method and flow-modulated comprehensive two-dimensional gas chromatography-triple quadrupole mass spectrometry.

J. Chromatogr. A, 1645 (2021) 462126.


51.  Mariosimone Zoccali, Tania Maria Grazia Salerno, Peter Q. Tranchida, Luigi Mondello.

Use Of A Low-Cost, Lab-Made Y-Interface For Liquid-Gas Chromatography Coupling For The Analysis Of Mineral Oils In Food Samples.

J. Chromatogr. A, 1648 (2021) 462191.


52.  Amandine Dispas, Adrian Clarke, Alexandre Grand-Guillaume Perrenoud, Luca Gioacchino Losacco, Jean-Luc Veuthey, Quentin Gros, Jérémy Molineau, Angéline Noireau, Caroline West, Fabio Salafia, Mariosimone Zoccali, Luigi Mondello, Amber Guillen, Jenny Wang, Kelly Zhang, Philipp Jochems, Gesa Schad, Kosuke Nakajima, Shinnosuke Horie, Jan Joseph, Maria Kristina Parr, Pierre Billemont, Antoni Severino, Sonja Schneider, Edgar Naegele, Daniel Kutscher, Rick Wikfors, Regina Black, Lee Ingvaldson, Jimmy Oliveira Da Silva, Raffeal Bennett, Erik L. Regalado, Thi Phuong Thuy Hoang, David Touboul, Yana Nikolova, Mariana Kamenova-Nacheva, Vladimir Dimitrov, Blair K. Berger, Kevin A. Schug, Solène Kerviel-Guillon, Fabien Mauge, Masatomo Takahashi, Yoshihiro Izumi, Takeshi Bamba, Florent Rouvière, Sabine Heinisch, Davy Guillarme, Philippe Hubert.

Interlaboratory study of a supercritical fluid chromatography methodfor the determination of pharmaceutical impurities: Evaluation ofmulti-systems reproducibility.

J. Pharmaceut. Biomed, 203 (2021) 114206.


53.  Santina Santisi, Mariosimone Zoccali, Valentina Catania, Paola Quatrini, Luigi Mondello, Maria Genovese, Simone Cappello.

Biodegradation Potential of Oil-degrading Bacteria Related to the Genus Thalassospira Isolated from Polluted Coastal Area in Mediterranean Sea.



54.  Alessia Arena, Mariosimone Zoccali, Alessandra Trozzi, Peter Q. Tranchida, Luigi Mondello.

Occurrence of Mineral Oil Hydrocarbons in Omega-3 Fatty Acid Dietary Supplements.

Foods 10, 2424, 2021.


55.  Mariosimone Zoccali, Marina Russo, Maria Rita Testa Camillo, Fabio Salafia, Peter Q. Tranchida, Paola Dugo, Luigi Mondello.

On-line coupling of supercritical fluid extraction with enantioselective supercritical fluid chromatography-triple quadrupole mass spectrometry for the determination of chiral pesticides in hemp seeds: A proof-of-principle study.

Food Chemistry 373 (2022) 131418.


56.  Paige E. Sudol, Micaela Galletta, Peter Q. Tranchida, Mariosimone Zoccali, Luigi Mondello, Robert E. Synovec.

Untargeted profiling and differentiation of geographical variants of wine samples using headspace solid-phase microextraction flow-modulated comprehensive two-dimensional gas chromatography with the support of tile-based Fisher ratio analysis.

J. Chromatogr. A 1662 (2022) 462735.


57.  Micaela Galletta, Mariosimone Zoccali, Nick Jones, Luigi Mondello, Peter Q. Tranchida.

Flow‑modulated comprehensive two‑dimensional gas chromatography combined with time‑of‑fight mass spectrometry: use of hydrogen as a more sustainable alternative to helium.

Anal. Bioanal. Chem. 2022.


58.  Adriana Arigò, Marina Russo, Maria Rita Testa Camillo, Paola Dugo, Luigi Mondello Mariosimone Zoccali.

Supercritical fluid chromatography‑tandem mass spectrometry of oxygen heterocyclic compounds in Citrus essential oils.

Anal. Bioanal. Chem. 414 (2022) 4821-4836. 


59.  Maria Grimaldi, Antonella Cavazza, Olimpia Pitirollo, Mariosimone Zoccali, Luigi Mondello, Daniele Giuffrida.

Analytical evaluation of carotenoids, apocarotenoids, capsaicinoids, and phenolics to assess the effect of a protective treatment on chili peppers dried at different temperatures.

Eur. Food Res. Technol. 414 (2022) 4821-4836. 

60.  Alessia Arena, Mariosimone Zoccali, Luigi Mondello, Peter Q. Tranchida.

Direct analysis of phthalate esters in vegetable oils by means of comprehensive two-dimensional gas chromatography combined with triple quadrupole mass spectrometry.

Food Chem. 396 (2022) 133721.


61.   Antonio Ferracane, Ivan Aloisi, Micaela Galletta, Mariosimone Zoccali, Peter Q. Tranchida, Luigi Mondello.

Automated sample preparation and fast GC–MS determination of fatty acids in blood samples and dietary supplements.

Anal. Bioanal. Chem. 414 (2022) 8423-8435.


62.  Alessia Arena, Mariosimone ZoccaliLuigi Mondello, Peter Q. Tranchida.

A method for the determination of 70 pesticides in extra virgin olive oil based on a limited‑volume solvent extraction step prior to comprehensive two‑dimensional gas chromatography‑tandem mass spectrometry.

Anal. Bioanal. Chem. (2022) doi: 10.1007/s00216-022-04494-6.


63.  Micaela Galletta, Mariosimone ZoccaliDonato Creti, Luigi Mondello, Peter Q. Tranchida.

A green and sustainable method for Capsicum volatilome investigation by means of headspace solid-phase microextraction combined with flow-modulated two-dimensional gas chromatography-mass spectrometry using hydrogen as carrier gas.

Green Anal. Chem. 4 (2023) 100050.